Experimental Propellant Vacuum Processing

Propellant Vacuum ProcessingExperimental Propellant Vacuum Processing My vacuum pump is a RobinAir 6cfm unit as seen above. I picked it up for $100 from a pawn shop. They seem to run $100-$140 +S&H on EBay. It's got ample capacity and one could likley do with a smaller one.

The only issue with the RobinAir is that it will mist a bit. By this I mean that the pump exhaust contains a small amount of ultra fine oil mist. It's not very noticable for short runs but should preclude running it inside one's house. Garage is OK. You can mitigate this to some extent by laying a rag over the handle assembly (which contains the vent). Don't plug the vent up, the pump isn't built for that, merely provide a rag that will catch most of the mist.On a long run, some oil film may run down the side of the motor adjacent to the exhaust hole.

With that caveat about misting, I otherwise must say that the RobinAir, particularly a used one, is an impressive value. This particular model will pull my mixing bowl down to 29+" Hg within a couple of seconds. You need to watch the initial surges until the propellant settles down. With this capacity (the 6cfm model), it's easy to set the vent ball valve to a partial setting to hold lower vacuums in the chamber to allow the propellant to settle without banging it or needing to watch it religiously.

Propellant Degassing Vacuum Valve Manifold

The plate is 1/2" Polycarbonate from U.S. Plastic Supply. I have another 3/4" plate from a friend.

The gasket is roofing rubber EDPM and is a piece of some I bought from Wickman as part of his rocket kit. It's got a rough pattern but with this pump sucks down fast and fine without any holding to start it. You can otherwise get it from well stocked home centers.

Quick Disconnect Vacuum Fitting for Propellant De-gassing

I came up with a quick-disconnect vacuum fitting for propellant degassing.. I had this 1/4" reinforced tubing (you can do with thinner) and it didn't suck down onto the tubing so I soldered in a compression ferrule and it sucks up nicely to it yet is easy to disconnect.